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coordination of technical aspects of type approval and identi cation of problems affecting type approval as results of validation and con icting interpretations of recommendations; resolution of technical problems with regard to type approval in different countries; organization of compatibility testing of mobiles in different networks to ensure adequacy of type approval; review of results of GSM validation activities and assessment of effects on implementation plans; review of system simulator activities through a speci c sub-group System Simulator Project Group (SSPG).

with Z 1 , Z 2 , . . . independent, identical distributed normal variates with distribution N (0, 1). The evolve component of the Hull White model is implemented in the ppf.model. hull white.monte carlo.evolve module as shown below.

10

By using Br nsted acids of known pKa values and by examining their influence on the reduction of Q, we can get some qualitative information about the base strengths of Q and Q2 . Recently, some quantitative studies have been carried out on this problem. For example, Niyazmbetov et al. [54 f ] studied the pKa values of dihydrofullerene, C60H2, and related species, by combining cyclic voltammetry, controlled-potential electrolysis and acid-base titrations. They got (or estimated) in DMSO a pKa of * 8.9 for C60H ; pKa1 and pKa2 of 4.7 and 16 for C60H2; pKa1, pKa2 and pKa3 of 9, * 9 and * 25 for C60H ; and pKa2, pKa3 and pKa4 of 16, * 16 3 and * 37 for C60H4. To obtain these estimates, they used a relation as in Eq. (8.4):

Further, the effect of local heating on the movement of metal atoms can be included in terms of the temperature dependence of the diffusion coef cient D in Eq. (5.3.2) given by D D0 e Ea = kT 5:3:4

0 0 255

also used in DMF and Py as oxidizing agent Fe(II), Cr(II) and Ti(III) in DMF can be determined by titration with Cu(II) When I is titrated with Cu(ClO4)2 in AN, it is oxidized in two steps, I I3 and I3 I2 The formal potentials of the two steps are + 0396 V and 0248 V vs Ag/Ag+, respectively Many organic compounds, such as hydroquinone, ascorbic acid, ferrocene and its derivatives, allylamine, hydroxylamine, phenylhydrazine, thiourea and SH compounds, can also be titrated with Cu(II) in AN Figure 49 shows the titration curves of tetramethylbenzidine (TMB) in AN [12] In dry AN, TMB is oxidized in two steps as follows: TMB Cu II 3 TMB Green Cu I TMB Green Cu II 3 TMB Orange2 Cu I In AN containing * 01 M water, however, the oxidation occurs in three steps.

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The reactions of the first two steps are the same as those above, and the third step corresponds to the oxidation of TMB H +, which is produced in the presence of water There are cases in which the titration curves are improved by the presence of water Figure 410 shows the titration curves of hydroquinone (HQ) Only in the presence of * 01 M water can the end-point be detected [13] Water acts as the acceptor of the proton, which is generated in the oxidation of HQ: Hydroquinone 2Cu II 2H2 O 3 Quinone 2Cu I 2H3 O 2 The titration with Cu(II) is also influenced by the anions of electrolytes, because the potential of the Cu(II)/Cu(I) couple changes by the complexation of anions with Cu(II) and Cu(I) The formal potential of the Fe(III)/Fe(II) couple in AN is + 157 V vs Ag/0.